![SYNTHESIS OF MONO [6A-O- (4-TOLYLSULPHONYL)] -β-CYCLODEXTRIN](/upload/a1160463316ae96644a303580cf6ab6c/issues/cover/fff7c2c8fa5459f7756c03885177f6c3.jpeg)
SYNTHESIS OF MONO [6A-O- (4-TOLYLSULPHONYL)] -Β-CYCLODEXTRIN
Rubrics: CHEMISTRY AND CHEMICAL TECHNOLOGY
Authors:
Type:
Article
Pages:
from 31
to 33
Status:
Published
Received:
10.03.2020
Accepted:
05.06.2020
Published:
05.06.2020
Subject area:
OKSO 04.04.02 Химия, физика и механика материалов
Language:
Russian
Keywords:
β-cyclodextrin, tosyl chloride, mono [6A-O- (4-tolylsulphonyl)]-β-cyclodextrin.
Abstract (English):
As a result of improvement of the preparation procedure of tosyl-β-cyclodextrin in aqueous alkaline medium by the interaction of β-cyclodextrin with tosyl chloride (TosCl) at low temperatures, the yield of the target product was increased from 38% to 58%.
As a result of improvement of the preparation procedure of tosyl-β-cyclodextrin in aqueous alkaline medium by the interaction of β-cyclodextrin with tosyl chloride (TosCl) at low temperatures, the yield of the target product was increased from 38% to 58%.
Keywords:
β-cyclodextrin, tosyl chloride, mono [6A-O- (4-tolylsulphonyl)]-β-cyclodextrin.
β-cyclodextrin, tosyl chloride, mono [6A-O- (4-tolylsulphonyl)]-β-cyclodextrin.
1. Modified Cyclodextrins for Chiral Separation: Modificftion of Cyclodextrin
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3. Muderawan I. W., Ong T. T., Lee T. C., Young D. J., Ching B.C., Ng S.C. //Tetrahedron Lett. 2005. V. 46. № 46. P. 7905-7907. doihttps://doi.org/10.1016/j.tetlet.2005.09.099.
